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Catecolaminas fraccionadas en orina por HPLC MS/MS
Flow cells for detection
We do offer two different flow cells for HPLC with electrochemical detection, each having unique features for specific applications. The SenCell is a new generation electrochemical flow cell specially designed for highest sensitivity. The FlexCell with its replaceable working electrode is specifically developed for applications with a gold or boron doped diamond electrode.
Read more about our flow cells for electrochemical detection:
- The SenCell for highest sensitivity
- High Sensitivity Flow Cell for UHPLC/ECD
- Adjustable Spacer Technology (AST)
- No spacers or gaskets
- Fast stabilization
- The SenCell™ is a new generation electrochemical flow cell specifically designed for highest sensitivity. The tool free assembly and the continuously adjustable working volume guarantee ease of use and fast stabilization. The effective volume of the cell – area above electrode – is small and can be adjusted between roughly 0 and 300 nL. Multiple working and reference electrodes are available making the cell ideally suited for use in (U)HPLC with Electrochemical Detection (ECD).
- On the right, a SenCell with integrated HyREF, a high pH compatible, reference electrode is shown. When opening the cell by the metal ring, the metal electrode is visible, that is in direct contact with mobile phase. No chemical coating or salt bridge is applied, which makes the reference electrode maintenance free!
SenCell with HyREF reference electrode.
Opening the cell shows the inlet block with integrated HyREF – a maintenance free reference electrode.
- The FlexCell with exchangeable working electrode
Highest sensitivity
To realize the highest detection sensitivity, the cell design is based on the confined wall-jet principle. The liquid flows perpendicular to the electrode surface, thus minimizing the diffusion layer. A three-electrode configuration is used consisting of working electrode (WE), reference electrode (REF) and auxiliary electrode (AUX). The AUX is kept at precisely the same potential as the reference electrode via a voltage clamp, compensating for any polarization effects that might occur at the electrodes. In addition, utmost care has been devoted to the quality and finishing of the electrode material so that the highest sensitivity with fast stabilization is achieved, making the cell ideally suited for ultra-trace analysis in (U)HPLC, micro- and capillary LC/ECD.
Wall-jet flow cell design. Solvent flow is perpendicular on the electrode surface.
Adjustable Spacer Technology – AST
The new design is using Adjustable Spacer Technology (AST), the use of polymeric gaskets (spacers) is now obsolete. The AST is a build-in micro-positioner for the working electrode relative to the inlet. To adjust the electrode position simply turn the micro-positioner mechanism in the cell with an adjustment key (included). By minimizing the electrode distance (‘spacer’), more signal will be ‘squeezed out’. For many applications this will improve the detection sensitivity.
Ease of use
The tool-free, easy-lock screw assembly allows for fast (dis-)assembly. Furthermore, the AST guarantees for highest sensitivity (S/N) and fast stabilization.
Adapter-kit for use with Coulochem II and III
Boost the sensitivity of your existing Coulochem detector (ESA) by making use of Antec’s SenCell. For easy installation an adapter-kit is available consisting of a Faraday cage (pn 250.4000) and Coulochem cell cable 250.0133 (II) or 250.0138 (III).
Adjustment from position 2 to 1: turn counterclockwise with the key.
Adjustment of the SenCell from position 3 to 0.5 results in a 2.5-fold increase in signal. Patented design: US Patent 2014/0102916 A1
Reference electrodes
The SenCell is available with 3 different color coded reference electrodes that can be easily exchanged to fit any application. The traditional salt bridge (Ag/AgCl) is blue. The more user-friendly ISAAC (In Situ Ag/AgCl) is green. The maintenance free, high pH inert HyREF is black.
IONICON PTR-TOF-MS - Trace VOC Analyzer
Sensitivity: > 200 cps/ppbv
Resolution: > 1500
LoD: < 10 pptv
Overview
Enter into the world of PTR-TOFMS with IONICON’s PTR-TOF 1000 and benefit from all the advantages only powerful time of flight based solutions offer:
- the entire mass range in split-seconds - no selection of masses - no waiting
- fast and sensitive for complex VOC mixtures and
- high mass resolution for better separation and identification.
More than a hundred PTR-TOF 1000 installations all over the planet are proof of its popularity and reliability. The PTR-TOF 1000 is the first choice for various international research campaigns but especially for 24/7 industrial monitoring or mobile air quality lab applications. It comes with a fully integrated IONICON data acquisition and data treatment software suite and can optionally be configured as automated VOC monitor with a customized substances identification library.
The PTR-TOF 1000 is our most affordable time PTR-TOF trace gas analyzer. Don't settle for anything less advanced, robust and reliable!
But wait, the PTR-TOF 1000 is just the beginning: expect up to 10x higher sensitivity with the PTR-TOF 1000 ultra.
Technical specifications
Mass resolution | > 1500 m/Δm (FWHM) for m/z > 79 |
Response time | < 100 ms |
Sensitivity | > 200 cps/ppbv for m/z 181 |
Detection limits | < 10 pptv for m/z 181 (averaged over 1 minute) |
Linearity range | 10 pptv - 1 ppmv |
Adjustable flow | 50 - 800 sccm |
Inlet system heating range | 40 - 180°C (2nd inlet system and other inlet options on request) |
Reaction chamber heating range | 40 - 120°C |
Weight | < 125 kg |
Dimensions (w x h x d) | 60x91x80 cm (23.7 x 35.9 x 31.5 in.) |
Power supply | 115/230 V, standby/typical operation: < 400/500-800 W |
Interfaces | -Touchscreen display 8x DI/O, 2x AI, 2x AO |
The sensor can be connected directly with the LNI Hydrogen Generators. When the hydrogen concentration detected exceeds a threshold of safety, the Hydrogen Generator automatically stops the production and audible and visual alarms will be reported.
Technical specifications
Models: 6940.00.050 |
6940.00.055 | |
Power Supply Voltage | 12 VDC +/- 5% |
Power Supply Current | 0.8 A use with 6940.00.056 |
Valve output | Open collector 12VDC/500mA |
Ambient temperature | 5-35°C (41-95°F) |
Ambient Humidity (max, non condensing) | 80% at 25°C (77°F) |
IP rating | IP20 |
6940.00.056 | |
Hydrogen Inlet pressure | 1 to 9 bar |
Inert Inlet pressure | 1 to 10 bar |
Pressure regulator | 1 to 9 bar |
6940.00.060 |
Hydrogen Sensitivity Range | 0.01% to 1.00% by hydrogen volume (25% LEL, Lower Explosion Limit) |
Accuracy | ± (5.0% of F.S. + 1000ppm) |
Typical Response Time | less than 20 sec |
Power Supply Voltage | From 9VDC to 28VDC |
Communication port | RS-485 |
Protocol | MODBUS-RTU |
Calibration Interval | 1 year (suggested 180 days) |
Hydrogen Sensor Technology | Dioxide semiconductor |
Product Life Expectancy | 10 years |
Body temperature range | -10 °C to 40 °C |
Flow cells for detection
We do offer two different flow cells for HPLC with electrochemical detection, each having unique features for specific applications. The SenCell is a new generation electrochemical flow cell specially designed for highest sensitivity. The FlexCell with its replaceable working electrode is specifically developed for applications with a gold or boron doped diamond electrode.
Read more about our flow cells for electrochemical detection:
- The SenCell for highest sensitivity
- High Sensitivity Flow Cell for UHPLC/ECD
- Adjustable Spacer Technology (AST)
- No spacers or gaskets
- Fast stabilization
- The SenCell™ is a new generation electrochemical flow cell specifically designed for highest sensitivity. The tool free assembly and the continuously adjustable working volume guarantee ease of use and fast stabilization. The effective volume of the cell – area above electrode – is small and can be adjusted between roughly 0 and 300 nL. Multiple working and reference electrodes are available making the cell ideally suited for use in (U)HPLC with Electrochemical Detection (ECD).
- On the right, a SenCell with integrated HyREF, a high pH compatible, reference electrode is shown. When opening the cell by the metal ring, the metal electrode is visible, that is in direct contact with mobile phase. No chemical coating or salt bridge is applied, which makes the reference electrode maintenance free!
SenCell with HyREF reference electrode.
Opening the cell shows the inlet block with integrated HyREF – a maintenance free reference electrode.
- The FlexCell with exchangeable working electrode
Highest sensitivity
To realize the highest detection sensitivity, the cell design is based on the confined wall-jet principle. The liquid flows perpendicular to the electrode surface, thus minimizing the diffusion layer. A three-electrode configuration is used consisting of working electrode (WE), reference electrode (REF) and auxiliary electrode (AUX). The AUX is kept at precisely the same potential as the reference electrode via a voltage clamp, compensating for any polarization effects that might occur at the electrodes. In addition, utmost care has been devoted to the quality and finishing of the electrode material so that the highest sensitivity with fast stabilization is achieved, making the cell ideally suited for ultra-trace analysis in (U)HPLC, micro- and capillary LC/ECD.
Wall-jet flow cell design. Solvent flow is perpendicular on the electrode surface.
Adjustable Spacer Technology – AST
The new design is using Adjustable Spacer Technology (AST), the use of polymeric gaskets (spacers) is now obsolete. The AST is a build-in micro-positioner for the working electrode relative to the inlet. To adjust the electrode position simply turn the micro-positioner mechanism in the cell with an adjustment key (included). By minimizing the electrode distance (‘spacer’), more signal will be ‘squeezed out’. For many applications this will improve the detection sensitivity.
Ease of use
The tool-free, easy-lock screw assembly allows for fast (dis-)assembly. Furthermore, the AST guarantees for highest sensitivity (S/N) and fast stabilization.
Adapter-kit for use with Coulochem II and III
Boost the sensitivity of your existing Coulochem detector (ESA) by making use of Antec’s SenCell. For easy installation an adapter-kit is available consisting of a Faraday cage (pn 250.4000) and Coulochem cell cable 250.0133 (II) or 250.0138 (III).
Adjustment from position 2 to 1: turn counterclockwise with the key.
Adjustment of the SenCell from position 3 to 0.5 results in a 2.5-fold increase in signal. Patented design: US Patent 2014/0102916 A1
Reference electrodes
The SenCell is available with 3 different color coded reference electrodes that can be easily exchanged to fit any application. The traditional salt bridge (Ag/AgCl) is blue. The more user-friendly ISAAC (In Situ Ag/AgCl) is green. The maintenance free, high pH inert HyREF is black.