TT24-7xr Markes International

Introducing the new TT24-7xr – an advanced, method-compliant thermal desorption (TD) system for continuous low-flow environmental monitoring of trace-level volatile and semi-volatile organic compounds (VOCs and SVOCs) by GC–MS.

The innovative dual-trap design enables 100% data capture, while unattended monitoring (ideal for mobile and unstaffed laboratories) is aided by cryogen-free operation and remote control of several systems from a single location.

Characteristics

1. Improved laboratory efficiency. Automated, unattended stream selection facilitates easy sequencing between the samples, blank and calibration standard channels at user-defined frequencies.

2. Precision of quantitative analyses. An optional internal standard accessory enables gas-phase internal standards to be introduced onto either focusing trap.

3. Platform-neutral. The short, heated transfer line allows the TT24-7xr to be installed on all major makes of GC and GC–MS.

4. Unparalleled analyte and concentration range. The inert, uniformly heated flow path ensures compatibility with C2–C40, including reactive species... from percent to sub-ppt concentrations.

5. Trouble-free sampling of humid air. The new Kori-xr water management module enables simultaneous sampling of C2 and polar VOCs, including monoterpenes.

Powerful options for method-compliant on-line monitoring

  •  Continuous on-line monitoring. The TT24-7xr achieves continuous on-line monitoring through the use of two cold traps working in tandem. Two focusing traps working in tandem provide complete data-capture for on-line sampling of air using the TT24-7xr. At the time-point illustrated, sampling is taking place onto Trap A, while Trap B is being desorbed (with a portion of the flow to the GC being directed to a re-collection tube).
  • Off-line analysis: In addition to on-line monitoring, sorbent tube analysis can be carried out on the TT24-7xr, making it suitable for a variety of air-monitoring scenarios.

  • Re-collection and method validation: The ability to perform tube analysis facilitates the quantitative recovery and re-collection of on-line samples for repeat analysis, enabling easier analyte and method validation.

  • Effective water management: When analysing humid air, the moisture must be removed before the gas flow reaches the GC column and detector, to avoid poor chromatography. However, some polar species and ultra-volatiles can be lost when using typical water‑management methods such as a Nafion™ dryer or trap dry-purge. The cryogen-free Kori-xr™ module addresses this problem by removing water from humid air prior to analyte focusing – allowing high-sensitivity analysis of polar species, oxygenates and monoterpenes, as well as all other typical VOCs. Use of the Kori-xr module with TT24-7xr provides excellent results for the analysis of a 100% RH, 65-component TO-15 standard containing polar and non-polar analytes.

 

System Features

  •  Dual-trap continuous monitoring – 100% data capture.
  • Operates cryogen-free – ideal for unattended remote-site operation over extended periods.

  • Two independent sample channels – one for each of the two cold traps.

  • Calibration channel – automated addition of calibration gas during sequence.

  • Blank channel – automated addition of blank sample during sequence.

  • Leak test – automated leak checks of all flow paths, including both traps, tube, and split.

  • Internal standard (optional) – enables addition of gas phase standard onto either cold trap.

  • Kori-xr™ (optional) – enables on-line removal of airborne humidity.

  • Wide range of sampling flows with quantitative trapping offers high sensitivity.

  • Inert, uniformly-heated flow path offers compatibility for C2–C40 compounds and reactive species.

  • Ultra-rapid trap desorption delivers narrow peaks, optimising sensitivity even under splitless analytical conditions.

  • Efficient desorption means no cross-contamination and excellent chromatographic resolution – eliminating false positives.

  • Enhanced splitting options to accommodate high-level samples.

  • Tube desorption option facilitates quantitative repeat analysis for easy validation of analyte recovery.

  • Small footprint – suitable for mobile laboratories.

  • Robust and low maintenance, including minimal gas consumption.

  • Versatile: Compatible with any make of GC, fast GC, and various real-time vapour detectors.