1260 Infinity Diode Array Detector

The Agilent 1260 Infinity Diode Array Detector (DAD) features a completely new optical design based on the Agilent Max-Light cartridge cell with optofluidic waveguides. With typical detector noise levels of <± 0.6 µAU/cm the revolutionary 6 cm flow cell gives up to 10 times higher sensitivity than the Agilent 1200 Series DAD and VWD detectors. Any compromising refractive index and thermal effects are almost completely eliminated, resulting in significantly less baseline drift for more reliable and precise peak integration. Multiple wavelength and full spectral detection with up to 80 Hz data rates allows precise identification, quantification and purity analysis at trace levels for ultra-fast LC separations.

  • Ultra sensitivity through revolutionary Agilent Max-Light cartridge cell with 60 mm optical path length (typically noise: <± 0.6 µAU)

  • Universal Agilent Max-Light cartridge standard cell with 10 mm optical path length provides high sensitivity (noise: <± 3 µAU)

  • Wide linear range (typically up to 2.5 AU) - for reliable, simultaneous quantification of primary compounds, by-products and impurities.

  • Upgrade option to 1200 Infinity HDR-DAD solution provides 30x wider linear range for samples with widely different concentration levels.

  • More reliable and robust peak integration process due through less baseline drift.

  • Full spectral detection up to 80 Hz for compound identification by spectral libraries or verification of the separation quality with peak purity analysis for conventional and ultrafast LC. Simultaneous detection of up to 8 signals for increased sensitivity and selectivity.

  • Radio frequency identification (RFID) tags for all flow cells and UV lamp provide new levels of data traceability by recording parameters such as cell dimensions, lamp usage, serial number etc.

  • Electronic temperature control (ETC) provides maximum baseline stability and practical sensitivity under fluctuating ambient temperature and humidity conditions.

  • Reference wavelength for elimination of background interference.

  • Early maintenance feedback (EMF) for continuous tracking of instrument usage in terms of lamp burn time with user-settable limits and feedback messages.

  • Extensive diagnostics, error detection and display with Instant Pilot controller and Agilent Lab Advisor software.

 

Specifications: 1260 Infinity Diode-Array Detector (G4212B)

Detector type

1024-element diode array

Light source

Deuterium

Number of signals

8

Maximum sampling rate

80 Hz (both spectra and signals)

Short-term noise

< ± 3 x 10-6 AU at 230/4 nm, slit width 4 nm,
TC 2 sec, ASTM with 10 mm Max-Light cartridge cell

Typically <±  0.6  x 10-6 AU/cm at 230/4 nm, slit width 4 nm,
TC 2 sec, ASTM with 60 mm Max-Light cartridge cell

Drift

< 0.5 x 10-3 AU/hr at 230 nm

Linearity

> 2.0 AU (5 %) at 265 nm
Typically 2.5 AU (5 %)

Wavelength range

190-640 nm

Wavelength accuracy

± 1 nm, self-calibration with deuterium lines

Slit width

 4 nm (fixed)

Diode width

~ 0.5 nm

Wavelength bunching

Programmable, 2 - 400 nm, in steps of 1 nm

Flow cells

  • Max-Light Cartridge Cell (Standard)
    10 mm, σV = 1.0 μL, with RFID tags
  • Max-Light Cartridge Cell (High Sensitivity)
    60 mm, σV = 4 μL, with RFID tags
  • Max-Light Cartridge Ultra Low Dispersion (ULD) Cell
    10 mm, σV = 0.6 μL, with RFID tags
  • Max-Light Cartridge High Dynamic Range (HDR) Cell
    3.7 mm, σV = 0.8 μL, with RFID tags

Maximum Operating Pressure (MPO) 1: 70 bar
Maximum Incidental Pressure (MIP) 2: 150 bar

1 Maximum operating pressure (MOP): Maximum pressure at which a system can operate continuously under normal conditions. 
2 Maximum incidental pressure (MIP): The maximum pressure which the system can experience during a short time.

Spectral tools

Data analysis software for spectra evaluation, including spectral libraries and peak purity functions

Analog output

Recorder/integrator: 100 mV or 1 V,
output range 0.001 – 2 AU, one output

Communications

Controller-area network (CAN),
RS-232C, APG Remote: ready
start, stop and shut-down
signals, LAN

GLP features

RFID for electronics records of flow cell and UV lamp conditions (path length, volume, product number, serial number, test passed, usage)
Early maintenance feedback (EMF) for continuous tracking of instrument usage in terms of lamp burn time with user settable limits and feedback messages. Electronic records of maintenance and errors. Verification of wavelength accuracy with deuterium lines.

Safety and maintenance

Extensive diagnostics, error detection and display (through Instant Pilot and Agilent Lab Advisor software), leak detection, safe leak handling, leak output signal for shutdown of pumping system. Low voltages in major maintenance areas.

Others

Electronic  temperature control (ETC) for complete optical unit

 

Specifications:  1260 Infinity Diode Array Detector VL (G1315D)

Detector type

1024-element diode array

Light source

Deuterium and tungsten

Number of signals

8

Maximum sampling rate

20 Hz

Short-term noise

< ± 0.7 x 10 -5 AU at 254/4 nm and at 750 nm, TC 2 sec.

Drift

< 0.9 x 10-3 AU/hr at 254 nm

Linearity

> 2.0 AU (5 %) at 265 nm

Wavelength range

190-950 nm

Wavelength accuracy

± 1 nm, self-calibration with deuterium lines
verification with holmium oxide filter

Slit width

Programmable: 1, 2, 4, 8, 16 nm

Diode width

< 1nm

Wavelength bunching

Programmable, 2 - 400 nm, in steps of 1 nm

Flow cells

Standard
13-µL volume, 10 mm-cell path length, 120 bar (1760 psi) pressure maximum
Semi-micro
5-µL volume, 6-mm cell path length, 120 bar (1760 psi) pressure maximum

Micro
2-µL, volume, 3-mm cell path length, 400 bar (5880 psi) pressure maximum
Semi-nano
500-nanoliter volume., 10-mm cell path length, 50 bar (735 psi) pressure maximum
Nano
80-nanoliter volume, 6-mm cell path length, 50 bar (735 psi) pressure maximum
High Pressure
1.7-µL volume, 6-mm cell path length, 400 bar (5880 psi) pressure maximum
Preparative 3 mm
3-mm cell path length, 120 bar (1760 psi) pressure maximum

Preparative 3 mm 
0.3-mm cell path lenght, 20 bar (294 psi) pressure maximum, quartz
Preparative 0.06 mm
0.06-mm cell path length, 20 bar (294 psi) pressure maximum, quartz

Time programmable

Wavelength, polarity, peak width, lamp bandwidth, autobalance, wavelength range, threshold, spectra storage mode

Spectral tools

Data analysis software for spectra evaluation, including spectral libraries and peak purity functions

Analog output

Recorder/integrator: 100 mV or 1 V, 2 outputs

Communications

LAN, Controller-area network (CAN),
RS-232C, APG Remote: ready start, stop and shut-down signals

GLP features

RFID for electronics records of flow cell and UV lamp conditions (path length, volume, product number, serial number, test passed, usage)
Early maintenance feedback (EMF) for continuous tracking of instrument usage in terms of lamp burn time with user settable limits and feedback messages. Electronic records of maintenance and errors. Verification of wavelength accuracy with built-in holmium oxide filter.

Safety and maintenance

Extensive diagnostics, error detection and display through Agilent Instant Pilot and Agilent Lab Advisor software. Leak detection, safe leak handling, and leak output signal for shutdown of pumping system. Low voltages in major maintenance areas.

Others

Electronic temperature control (ETC) for the complete optical unit