1290 Infinity II Diode Array Detector

World’s most sensitive and fastest diode-array detector
 
The Agilent 1290 Infinity Diode Array Detector (DAD) is the world`s most sensitive diode-array detector and features a completely new optical design based on the Agilent Max-Light cartridge cell with optofluidic waveguides. With typical detector noise levels of < ± 0.6 µAU/cm the revolutionary 6 cm flow cell gives up to 10 times higher sensitivity than the 1200 Series DAD and VWD. Any compromising refractive index and thermal effects are almost completely eliminated, resulting in significantly less baseline drift for more reliable and precise peak integration. For ultra high productivity the 1290 Infinity DAD offers multiple wavelength and full spectral detection at sampling rates up to 160 Hz

- Universal Agilent Max-Light standard cartridge cell with 10 mm optical path length provides high sensitivity (noise: < ± 3 µAU) and low peak dispersion for 2.1, 3 and 4.6 mm id columns.

- Programmable slit from 1 to 8 nm provides optimum incident light conditions for rapid optimization of sensitivity, linearity and spectral resolution.

- Multiple wavelength and full spectral detection at high sampling rate of 240 Hz, keeping pace with fastest possible analysis speed.

- More reliable and robust peak integration process due through less baseline drift.

- Full spectral detection for compound identification by spectral libraries or verification of the separation quality with peak purity analysis for ultrafast LC. Simultaneous detection of up to 8 signals for increased sensitivity and selectivity.

- Wide linear range (typically up to 2.5 AU) - for reliable, simultaneous quantification of primary compounds, by-products and impurities.

- Upgrade option to 1290 Infinity II HDR DAD solution provides 30x wider linear range for samples with widely different concentration levels. More details

- Radio frequency identification (RFID) technology for flow cells and lamp provide new levels of data security and traceability.

- Next generation of electronic temperature control (ETC) provides maximum baseline stability and practical sensitivity under fluctuating ambient temperature and humidity conditions

Specifications: 1290 Infinity Diode-Array Detector (G4212A)

Detector type

1024-element diode array

Light source

Deuterium

Number of signals

8

Maximum sampling rate

160 Hz (both spectra and signals)

Short-term noise

< ± 3 x 10-6 AU at 230/4 nm, slit width 4 nm, 
TC 2 sec, ASTM with 10 mm Max-Light cartridge cell

Typically <± 0.6 x 10-6 AU/cm at 230/4 nm, slit width 4 nm, 
TC 2 sec, ASTM with 60 mm Max-Light cartridge cell

Drift

< 0.5 x 10-3 AU/hr at 230 nm

Linearity

> 2.0 AU (5 %) at 265 nm
Typically 2.5 AU (5 %)

Wavelength range

190-640 nm

Wavelength accuracy

± 1 nm, self-calibration with deuterium lines

Slit width

Programmable: 1, 2, 4, 8 nm

Diode width

~ 0.5 nm

Wavelength bunching

Programmable, 2 - 400 nm, in steps of 1 nm

Flow cells

Max-Light Cartridge Cell (Standard)
10 mm, σV = 1.0 μL, with RFID tags 
Max-Light Cartridge Cell (High Sensitivity)
60 mm, σV = 4 μL, with RFID tags 
Max-Light Cartridge Ultra Low Dispersion (ULD) Cell
10 mm, σV = 0.6 μL, with RFID tags 
Max-Light Cartridge High Dynamic Range (HDR) Cell
3.7 mm, σV = 0.8 μL, with RFID tags

Maximum Operating Pressure (MPO) 1: 70 bar
Maximum Incidental Pressure (MIP) 2: 150 bar
1 Maximum operating pressure (MOP): Maximum pressure at which a system can operate continuously under normal conditions. 
2 Maximum incidental pressure (MIP): The maximum pressure which the system can experience during a short time.

Spectral tools

Data analysis software for spectra evaluation, including spectral libraries and peak purity functions

Analog output

Recorder/integrator: 100 mV or 1 V, output range 0.001 – 2 AU, one output

Communications

LAN, controller-area network (CAN), RS-232C, APG Remote: ready start, stop and shut-down signals

GLP features

RFID for electronics records of flow cell and UV lamp conditions (path length, volume, product number, serial number, test passed, usage)

Early maintenance feedback (EMF) for continuous tracking of instrument usage in terms of lamp burn time with user settable limits and feedback messages. Electronic records of maintenance and errors. Verification of wavelength accuracy with deuterium lines.

Safety and maintenance

Extensive diagnostics, error detection and display through Agilent Instant Pilot and Agilent Lab Advisor software. Leak detection, safe leak handling, leak output signal for shutdown of pumping system. Low voltages in major maintenance areas.

Others

Electronic temperature control (ETC) for the complete optical unit